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- Publisher
- Royal Society of Chemistry
- Copyright
- This journal is © The Royal Society of Chemistry
- ISSN
- 1477-9226
- eISSN
- 1477-9234
- DOI
- 10.1039/b704327a
- pmid
- 17622419
- Publisher site
- See Article on Publisher Site
Abstract
The hydrothermal reaction of Cu(NO), isophthalate (ip) and 2,2′-bipyridine (2,2′-bpy) without or with KCrO affords different complexes, whose structures are controlled only by the addition of the KCrO. The reaction of Cu(NO), isophthalate and 2,2′-bipyridine yields a novel one-dimensional double-chain coordination polymer [Cu(ip)(Hipa)(bpy)] (). However, with the addition of KCrO in the above reaction at the same hydrothermal conditions, a discrete hexanuclear Cu() complex [Cu(ipO)(2,2′-bpy)(HO)]·6HO () (ipOH = 2-hydroxyisophthalate) was isolated. It is interesting to find that the reaction of isophthalate (ip) oxidized to 2-hydroxyisophthalate (ipOH) occurs. KCrO acts as an oxidant. The magnetic properties of and have been investigated by variable-temperature magnetic susceptibility and magnetization measurements, and the results reveal that intramolecular ferromagnetic interactions exist with weak intermolecular antiferromagnetic interactions at very low temperature in and weak antiferromagnetic interactions admixture with strong ferromagnetic interactions in .
Journal
Dalton Transactions – Royal Society of Chemistry
Published: Jul 10, 2007